Find the most up-to-date version of ASTM E at Engineering Macroetching, also known as deep etching, involves etching specimens prepared with a suitable acid or reagent for macrostructural examination. Contact us. Purchase your copy of ASTM E – 17 as a PDF download or hard copy directly from the official BSI Shop. All BSI British Standards available.

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Overetching can lead to misinterpretation. Photographs for Rating Macroetched Steel 3 plates 3 3. Examination and rating of specimens e3811 be in accordance with Sections 10 and 11 of this E standard.

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Maintain a sufficient volume of solution in the vessel to cover the specimen with a layer of at least 25 mm 1 in. The etching solution may be reused if it has not become excessively contaminated or weakened. This is especially true for sulfuric acid. Compositional differences also in? The hydrochloric acid need not be reagent grade. Examination of Continuously Cast Product Specimens With reductions over a 3: The etching solution should be clear and free from scum.

Significance and Use 4.

It may be necessary to use solvents to clean the surface. Sharp tools are necessary to produce a good specimen. A number in parentheses indicates the year of last reapproval.

This standard is subject to revision at any time by the responsible technical committee and must be reviewed every?

In the case of forgings, depending upon prior agreement, this may be accomplished r381 adding excess metal for discard on the ends or ends of the forging; or, by forging in multiple lengths and removing the test disk between individual pieces when cutting up the multiple forging. The acids are strong and they can cause serious chemical burns.

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Macroetch Examinations

When the use of a reagent other than those described in 5. Remove the smut that forms on the specimen surface by scrubbing the surface with a stiff brush under hot running water. Evaluation of machined parts for grinding cracks in tools and dies. 3e81 is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

A freshly made solution is necessary for best results. Precision and Bias Last previous edition approved in as E — This will generate a smooth surface and remove cold work from prior operations.

The type of condition present may be identi?

Enter your personal account email address to request a password reset: Macroetching, also known as deep etching, involves etching specimens prepared with a suitable acid or reagent for macrostructural examination at low magnifications and rating by a grades series of photographs showing the incidence of certain conditions such as: Inspection is most effective when done while the piece is still wet. The solution may be heated without serious change in concentration.

The method is limited in application to bars, billets, blooms, and forgings of carbon and low alloy steels. The use of this reagent necessitates a smooth surface. These may be located anywhere from the near surface region of the product to the center of the product, depending on the source and severity of the condition.

The name implies that the etched surface is examined visually, or at low magni? E — 01 5. Sulfur printing shall be performed in accordance with Practice E Disks may be faced on a lathe or a shaper. Land Use and Development. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. If you feel that your comments have not received a fair hearing you should make your views known to the ASTM Committee on Standards, at the address shown below.

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In most cases, 15 to 30 min will be sufficient for hot-acid etching. Sufficient torch cut material should be removed by cold cutting to eliminate the thermal effects of torch cutting.

Macroetching Examinations – ASTM E & ASTM E Testing | SGS MSi Testing

Plate III is used to identify the type of condition observed on the macroetch specimens. The reagent is used at room temperature by immersion or swabbing. See the specific precautionary statement in 5.

Torch cutting or other hot cutting will materially affect the structure of the specimen and may be used only when necessary to remove a larger piece prior to cutting asym size by cold methods. Enter your account email address to request a password reset: Small xstm may be etched in glass or porcelain vessels of the types commonly available in laboratories.

Go to Navigation Go to Content. After the smut is removed, rinse the specimen under hot running water and blow it dry with compressed air. The reagent should be used under a fume asgm, or some other means of carrying off the corrosive fumes must be provided. Search book title Enter keywords for book title search. Are you sure you want to asgm the cart? They are also known as shatter cracks or hairline cracks. This should be added to an etching bath that is operating at room temperature.

Billets or blooms going into small sizes are sampled after the initial breakdown.

Last modified: January 16, 2020